Two-step synthesis of CdS (hcp) nanorods using sonochemical and hydrothermal processes
CdS (hcp) crystals were synthesized using CdCl 2.2H 2O in C 4H 11N containing 20% (NH 4) 2S by the 5 h sonochemical process followed by the hydrothermal rea...
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| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
2014
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| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-78249246321&partnerID=40&md5=de3b462e29cc61ede3b95ec578b6b7b8 http://cmuir.cmu.ac.th/handle/6653943832/6222 |
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| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | CdS (hcp) crystals were synthesized using CdCl
2.2H
2O in C
4H
11N containing 20% (NH
4)
2S by the 5 h sonochemical process followed by the hydrothermal reaction at different temperatures and times. CdS (hcp) crystals composing of Cd and S were detected using XRD, SAED and EDX. A Raman spectrometer revealed the presence of fundamental and overtone modes at 299 and 596 cm
-1, respectively. The crystals are nanorods growing in systematic array analyzed using TEM and HRTEM. Their photoluminescence is in the blue spectral region at 409-422 nm (2.94-3.03 eV). |
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