Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
Bi2S3 nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3 has the orthorhombi...
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| التنسيق: | مقال |
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2014
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| الوصول للمادة أونلاين: | http://www.scopus.com/inward/record.url?eid=2-s2.0-77954217737&partnerID=40&md5=5e9dd2949ac6ab093b4aefea4d1c3608 http://cmuir.cmu.ac.th/handle/6653943832/6249 |
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| المؤسسة: | Chiang Mai University |
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th-cmuir.6653943832-62492014-08-30T03:24:00Z Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles Thongtem T. Pilapong C. Kavinchan J. Phuruangrat A. Thongtem S. Bi2S3 nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3 has the orthorhombic phase and appears as nanorods in flower-shaped bundles. A transmission electron microscopic (TEM) study reveals the independent single Bi2S3 nanorods with their growth along the [0 0 1] direction. A possible formation mechanism of Bi 2S3 nanorods in flower-shaped bundles is also proposed and discussed. Their UVvis spectrum shows the absorbance at 596 nm, with its direct energy band gap of 1.82 eV. © 2009 Elsevier B.V. 2014-08-30T03:24:00Z 2014-08-30T03:24:00Z 2010 Article 9258388 10.1016/j.jallcom.2010.03.240 JALCE http://www.scopus.com/inward/record.url?eid=2-s2.0-77954217737&partnerID=40&md5=5e9dd2949ac6ab093b4aefea4d1c3608 http://cmuir.cmu.ac.th/handle/6653943832/6249 English |
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Chiang Mai University |
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Chiang Mai University Library |
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Thailand |
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CMU Intellectual Repository |
| language |
English |
| description |
Bi2S3 nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3 has the orthorhombic phase and appears as nanorods in flower-shaped bundles. A transmission electron microscopic (TEM) study reveals the independent single Bi2S3 nanorods with their growth along the [0 0 1] direction. A possible formation mechanism of Bi 2S3 nanorods in flower-shaped bundles is also proposed and discussed. Their UVvis spectrum shows the absorbance at 596 nm, with its direct energy band gap of 1.82 eV. © 2009 Elsevier B.V. |
| format |
Article |
| author |
Thongtem T. Pilapong C. Kavinchan J. Phuruangrat A. Thongtem S. |
| spellingShingle |
Thongtem T. Pilapong C. Kavinchan J. Phuruangrat A. Thongtem S. Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| author_facet |
Thongtem T. Pilapong C. Kavinchan J. Phuruangrat A. Thongtem S. |
| author_sort |
Thongtem T. |
| title |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_short |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_full |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_fullStr |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_full_unstemmed |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_sort |
microwave-assisted hydrothermal synthesis of bi2s3 nanorods in flower-shaped bundles |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-77954217737&partnerID=40&md5=5e9dd2949ac6ab093b4aefea4d1c3608 http://cmuir.cmu.ac.th/handle/6653943832/6249 |
| _version_ |
1681420578276245504 |