Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction
AgBiS2 nanostructured flowers were produced from CH3COOAg, Bi(NO3)3.5H2O and thiosemicarbazide (NH2CSNHNH2) using different solvents [ethylene glycol (EG), water (H2O), polyethylene glycol with molecular weight of 200 (PEG200), and propylene glycol (PG)] in Teflon-lined stainless steel autoclaves. T...
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th-cmuir.6653943832-63042014-08-30T03:24:04Z Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction Thongtem T. Tipcompor N. Thongtem S. AgBiS2 nanostructured flowers were produced from CH3COOAg, Bi(NO3)3.5H2O and thiosemicarbazide (NH2CSNHNH2) using different solvents [ethylene glycol (EG), water (H2O), polyethylene glycol with molecular weight of 200 (PEG200), and propylene glycol (PG)] in Teflon-lined stainless steel autoclaves. The phase and purity were detected using X-ray diffraction (XRD), controlled by the solvents. The product was purified AgBiS2 produced by the 200 °C and 24 h reaction in EG, corresponding to selected area electron diffraction (SAED) and simulation patterns. Scanning and transmission electron microscopies (SEM and TEM) revealed the formation of nanostructured flowers - enlarged by the increase in the lengths of time and temperature. Their photoluminescence (PL) emissions were detected at the same wavelength of 382 nm (3.24 eV), although they were produced under different conditions. © 2010 Elsevier B.V. All rights reserved. 2014-08-30T03:24:04Z 2014-08-30T03:24:04Z 2010 Article 0167577X 10.1016/j.matlet.2010.01.003 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-75749097711&partnerID=40&md5=6ea33902d5d8a0fac3398c4bf4e24c2a http://cmuir.cmu.ac.th/handle/6653943832/6304 English |
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AgBiS2 nanostructured flowers were produced from CH3COOAg, Bi(NO3)3.5H2O and thiosemicarbazide (NH2CSNHNH2) using different solvents [ethylene glycol (EG), water (H2O), polyethylene glycol with molecular weight of 200 (PEG200), and propylene glycol (PG)] in Teflon-lined stainless steel autoclaves. The phase and purity were detected using X-ray diffraction (XRD), controlled by the solvents. The product was purified AgBiS2 produced by the 200 °C and 24 h reaction in EG, corresponding to selected area electron diffraction (SAED) and simulation patterns. Scanning and transmission electron microscopies (SEM and TEM) revealed the formation of nanostructured flowers - enlarged by the increase in the lengths of time and temperature. Their photoluminescence (PL) emissions were detected at the same wavelength of 382 nm (3.24 eV), although they were produced under different conditions. © 2010 Elsevier B.V. All rights reserved. |
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Article |
author |
Thongtem T. Tipcompor N. Thongtem S. |
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Thongtem T. Tipcompor N. Thongtem S. Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction |
author_facet |
Thongtem T. Tipcompor N. Thongtem S. |
author_sort |
Thongtem T. |
title |
Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction |
title_short |
Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction |
title_full |
Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction |
title_fullStr |
Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction |
title_full_unstemmed |
Characterization of AgBiS2 nanostructured flowers produced by solvothermal reaction |
title_sort |
characterization of agbis2 nanostructured flowers produced by solvothermal reaction |
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2014 |
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http://www.scopus.com/inward/record.url?eid=2-s2.0-75749097711&partnerID=40&md5=6ea33902d5d8a0fac3398c4bf4e24c2a http://cmuir.cmu.ac.th/handle/6653943832/6304 |
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