XPS characterization of perovskite relaxor PNN ceramics prepared by corundum precursor method

Perovskite ferroelectric PNN ceramics have been obtained from oxides by sintering in air, using a two-stage process with corundum Ni4Nb 2O9 precursor. Under suitable firing condition, XRD analysis revealed that the ceramics consist of 100% perovskite phase. The SEM, EDX, and XPS techniques were empl...

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Bibliographic Details
Main Authors: Srisombat L., Khamman O., Yimnirun R., Ananta S., Lee T.R.
Format: Conference or Workshop Item
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-75749133211&partnerID=40&md5=fbe51269bef960af208a4447634e4300
http://cmuir.cmu.ac.th/handle/6653943832/6334
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Institution: Chiang Mai University
Language: English
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Summary:Perovskite ferroelectric PNN ceramics have been obtained from oxides by sintering in air, using a two-stage process with corundum Ni4Nb 2O9 precursor. Under suitable firing condition, XRD analysis revealed that the ceramics consist of 100% perovskite phase. The SEM, EDX, and XPS techniques were employed to investigate the chemical composition of the surfaces of the PNN ceramics. Fluctuation in chemical composition, precipitation of NiO and the Pb-Ni-Nb-O phase different from perovskite were found. © (2010) Trans Tech Publications.