Characterization of Bi2S3 with different morphologies synthesized using microwave radiation

Characterization of Bi2S3 with different morphologies synthesized using microwave radiation

Bi2S3 with different morphologies (nanoparticles, nanorods and nanotubes) was synthesized using bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and two kinds of sulfur sources (CH3CSNH2 and NH2CSNH2) in different solvents (water, ethylene glycol and propylene glycol) via a microwave radiation method at...

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Main Authors: Thongtem T., Phuruangrat A., Wannapop S., Thongtem S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-70449534600&partnerID=40&md5=9fcf467f02c905013e0901be98473de7
http://cmuir.cmu.ac.th/handle/6653943832/6359
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Institution: Chiang Mai University
Language: English
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spelling th-cmuir.6653943832-63592014-08-30T03:24:07Z Characterization of Bi2S3 with different morphologies synthesized using microwave radiation Thongtem T. Phuruangrat A. Wannapop S. Thongtem S. Bi2S3 with different morphologies (nanoparticles, nanorods and nanotubes) was synthesized using bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and two kinds of sulfur sources (CH3CSNH2 and NH2CSNH2) in different solvents (water, ethylene glycol and propylene glycol) via a microwave radiation method at 180 W for 20 min. X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) indicated that all of the products are orthorhombic Bi2S3 phase of nanoparticles, nanorods and nanotubes, influenced by the sulfur sources and solvents. Formation mechanisms of the products with different morphologies are also proposed. © 2009 Elsevier B.V. All rights reserved. 2014-08-30T03:24:07Z 2014-08-30T03:24:07Z 2010 Article 0167577X 10.1016/j.matlet.2009.10.006 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-70449534600&partnerID=40&md5=9fcf467f02c905013e0901be98473de7 http://cmuir.cmu.ac.th/handle/6653943832/6359 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description Bi2S3 with different morphologies (nanoparticles, nanorods and nanotubes) was synthesized using bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) and two kinds of sulfur sources (CH3CSNH2 and NH2CSNH2) in different solvents (water, ethylene glycol and propylene glycol) via a microwave radiation method at 180 W for 20 min. X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) indicated that all of the products are orthorhombic Bi2S3 phase of nanoparticles, nanorods and nanotubes, influenced by the sulfur sources and solvents. Formation mechanisms of the products with different morphologies are also proposed. © 2009 Elsevier B.V. All rights reserved.
format Article
author Thongtem T.
Phuruangrat A.
Wannapop S.
Thongtem S.
spellingShingle Thongtem T.
Phuruangrat A.
Wannapop S.
Thongtem S.
Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
author_facet Thongtem T.
Phuruangrat A.
Wannapop S.
Thongtem S.
author_sort Thongtem T.
title Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_short Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_full Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_fullStr Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_full_unstemmed Characterization of Bi2S3 with different morphologies synthesized using microwave radiation
title_sort characterization of bi2s3 with different morphologies synthesized using microwave radiation
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-70449534600&partnerID=40&md5=9fcf467f02c905013e0901be98473de7
http://cmuir.cmu.ac.th/handle/6653943832/6359
_version_ 1681420599083139072

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