The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method

Nanostructured ZnS (hexagonal and cubic) were synthesized by a 200 °C and 24 h solvothermal reaction of Zn (CH3COO)2· 2H2O and L-cysteine (C3H7NO2S) in water, propylene glycol (PG) and glycerol (GR) solvents. The products, characterized by XRD, were specified as pure ZnS (hexagonal) in water, and Zn...

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Main Authors: Kaowphong S., Thongtem T., Yayapao O., Thongtem S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-80051783190&partnerID=40&md5=2069de8cd64696e026a18090e632101e
http://cmuir.cmu.ac.th/handle/6653943832/6418
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spelling th-cmuir.6653943832-64182014-08-30T03:24:11Z The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method Kaowphong S. Thongtem T. Yayapao O. Thongtem S. Nanostructured ZnS (hexagonal and cubic) were synthesized by a 200 °C and 24 h solvothermal reaction of Zn (CH3COO)2· 2H2O and L-cysteine (C3H7NO2S) in water, propylene glycol (PG) and glycerol (GR) solvents. The products, characterized by XRD, were specified as pure ZnS (hexagonal) in water, and ZnS (cubic) in PG and GR. SEM and TEM analyses showed the particle sizes and agglomerated behaviors, mainly related to the reaction media, which were in accordance with BET adsorption of nitrogen, with blue shift energy gaps relative to the bulk. © 2011 Elsevier B.V. All rights reserved. 2014-08-30T03:24:11Z 2014-08-30T03:24:11Z 2011 Article 0167577X 10.1016/j.matlet.2011.07.079 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-80051783190&partnerID=40&md5=2069de8cd64696e026a18090e632101e http://cmuir.cmu.ac.th/handle/6653943832/6418 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description Nanostructured ZnS (hexagonal and cubic) were synthesized by a 200 °C and 24 h solvothermal reaction of Zn (CH3COO)2· 2H2O and L-cysteine (C3H7NO2S) in water, propylene glycol (PG) and glycerol (GR) solvents. The products, characterized by XRD, were specified as pure ZnS (hexagonal) in water, and ZnS (cubic) in PG and GR. SEM and TEM analyses showed the particle sizes and agglomerated behaviors, mainly related to the reaction media, which were in accordance with BET adsorption of nitrogen, with blue shift energy gaps relative to the bulk. © 2011 Elsevier B.V. All rights reserved.
format Article
author Kaowphong S.
Thongtem T.
Yayapao O.
Thongtem S.
spellingShingle Kaowphong S.
Thongtem T.
Yayapao O.
Thongtem S.
The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method
author_facet Kaowphong S.
Thongtem T.
Yayapao O.
Thongtem S.
author_sort Kaowphong S.
title The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method
title_short The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method
title_full The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method
title_fullStr The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method
title_full_unstemmed The effect of solvents on ZnS nanostructures synthesized by biomolecule-assisted solvothermal method
title_sort effect of solvents on zns nanostructures synthesized by biomolecule-assisted solvothermal method
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-80051783190&partnerID=40&md5=2069de8cd64696e026a18090e632101e
http://cmuir.cmu.ac.th/handle/6653943832/6418
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