Influence of sintering temperature on densification and microstructure of Zn3Nb2O8 ceramics derived from nanopowders

Zinc niobate, Zn3Nb2O8, dielectric ceramics were fabricated by sintering Zn3Nb2O8 nanopowders derived from a rapid vibro-milling technique at various temperatures. Phase formation, densification, microstructure and dielectric properties of the ceramics were investigated as a function of sintering te...

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Bibliographic Details
Main Authors: Pakawanit P., Ananta S.
Format: Conference or Workshop Item
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-79952563177&partnerID=40&md5=66397b11289d5ebfb0b41c084e98151f
http://cmuir.cmu.ac.th/handle/6653943832/6590
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Institution: Chiang Mai University
Language: English
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Summary:Zinc niobate, Zn3Nb2O8, dielectric ceramics were fabricated by sintering Zn3Nb2O8 nanopowders derived from a rapid vibro-milling technique at various temperatures. Phase formation, densification, microstructure and dielectric properties of the ceramics were investigated as a function of sintering temperatures (1000-1200°C), using a combination of X-ray diffraction, Archimedes density measurement, scanning electron microscopy and dielectric measurement, respectively. It has been found that single-phase Zn 3Nb2O8 ceramics with maximum density of ∼98% theoretical density can be successfully produced with appropriate firing temperature, without any firing additives. Moreover, it is seen that the dielectric properties are found to enhance with increasing sintering temperature and grain size. © (2011) Trans Tech Publications.