Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent

Nanostructured Cu3BiS3 dendrites were successfully synthesized from CuCl, BiCl3 and L-cysteine in ethylene glycol (EG), using cyclic microwave radiation (CMR). The phase was detected by X-ray diffraction (XRD) and selected area electron diffraction (SAED), and was in accordance with that obtained by...

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Main Authors: Aup-Ngoen K., Thongtem S., Thongtem T.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-78649323463&partnerID=40&md5=76660ac280865255e05ec0168d884abe
http://cmuir.cmu.ac.th/handle/6653943832/6615
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Institution: Chiang Mai University
Language: English
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spelling th-cmuir.6653943832-66152014-08-30T03:24:24Z Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent Aup-Ngoen K. Thongtem S. Thongtem T. Nanostructured Cu3BiS3 dendrites were successfully synthesized from CuCl, BiCl3 and L-cysteine in ethylene glycol (EG), using cyclic microwave radiation (CMR). The phase was detected by X-ray diffraction (XRD) and selected area electron diffraction (SAED), and was in accordance with that obtained by the simulation. Scanning and transmission electron microscopic (SEM and TEM) techniques revealed the gradual transformation of nanoparticles to nanostructured dendrites, due to the increase of microwave power. Photoluminescence of Cu3BiS3 dendrites was a blue emission centered at 367 nm. © 2010 Elsevier B.V. All rights reserved. 2014-08-30T03:24:24Z 2014-08-30T03:24:24Z 2011 Article 0167577X 10.1016/j.matlet.2010.10.047 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-78649323463&partnerID=40&md5=76660ac280865255e05ec0168d884abe http://cmuir.cmu.ac.th/handle/6653943832/6615 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description Nanostructured Cu3BiS3 dendrites were successfully synthesized from CuCl, BiCl3 and L-cysteine in ethylene glycol (EG), using cyclic microwave radiation (CMR). The phase was detected by X-ray diffraction (XRD) and selected area electron diffraction (SAED), and was in accordance with that obtained by the simulation. Scanning and transmission electron microscopic (SEM and TEM) techniques revealed the gradual transformation of nanoparticles to nanostructured dendrites, due to the increase of microwave power. Photoluminescence of Cu3BiS3 dendrites was a blue emission centered at 367 nm. © 2010 Elsevier B.V. All rights reserved.
format Article
author Aup-Ngoen K.
Thongtem S.
Thongtem T.
spellingShingle Aup-Ngoen K.
Thongtem S.
Thongtem T.
Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent
author_facet Aup-Ngoen K.
Thongtem S.
Thongtem T.
author_sort Aup-Ngoen K.
title Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent
title_short Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent
title_full Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent
title_fullStr Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent
title_full_unstemmed Cyclic microwave-assisted synthesis of Cu3BiS3 dendrites using L-cysteine as a sulfur source and complexing agent
title_sort cyclic microwave-assisted synthesis of cu3bis3 dendrites using l-cysteine as a sulfur source and complexing agent
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-78649323463&partnerID=40&md5=76660ac280865255e05ec0168d884abe
http://cmuir.cmu.ac.th/handle/6653943832/6615
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