Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
Cubic and star-shaped dendritic PbS structures were successfully synthesized by the 120 °C and 10 h solvothermal reactions of lead nitrate and sulfur sources (thiourea and thiosemicarbazide). XRD, SEM and TEM analyses revealed the presence of pure cubic PbS phase with different morphologies, control...
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2014
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th-cmuir.6653943832-67332014-08-30T03:51:10Z Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method Phuruangrat A. Thongtem T. Kuntalue B. Thongtem S. Cubic and star-shaped dendritic PbS structures were successfully synthesized by the 120 °C and 10 h solvothermal reactions of lead nitrate and sulfur sources (thiourea and thiosemicarbazide). XRD, SEM and TEM analyses revealed the presence of pure cubic PbS phase with different morphologies, controlled by the sulfur sources. Cubic and star-shaped dendritic PbS crystals were respectively synthesized in the solutions containing thiourea and thiosemicarbazide as sulfur sources. Possible formation mechanisms of cubic and star-shaped dendritic PbS structures were also proposed. © 2012 Elsevier B.V. All rights reserved. 2014-08-30T03:51:10Z 2014-08-30T03:51:10Z 2012 Article 0167577X 10.1016/j.matlet.2012.04.129 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-84862158360&partnerID=40&md5=d727f2516407a6edc52bb0a46df11109 http://cmuir.cmu.ac.th/handle/6653943832/6733 English |
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Cubic and star-shaped dendritic PbS structures were successfully synthesized by the 120 °C and 10 h solvothermal reactions of lead nitrate and sulfur sources (thiourea and thiosemicarbazide). XRD, SEM and TEM analyses revealed the presence of pure cubic PbS phase with different morphologies, controlled by the sulfur sources. Cubic and star-shaped dendritic PbS crystals were respectively synthesized in the solutions containing thiourea and thiosemicarbazide as sulfur sources. Possible formation mechanisms of cubic and star-shaped dendritic PbS structures were also proposed. © 2012 Elsevier B.V. All rights reserved. |
| format |
Article |
| author |
Phuruangrat A. Thongtem T. Kuntalue B. Thongtem S. |
| spellingShingle |
Phuruangrat A. Thongtem T. Kuntalue B. Thongtem S. Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method |
| author_facet |
Phuruangrat A. Thongtem T. Kuntalue B. Thongtem S. |
| author_sort |
Phuruangrat A. |
| title |
Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method |
| title_short |
Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method |
| title_full |
Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method |
| title_fullStr |
Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method |
| title_full_unstemmed |
Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method |
| title_sort |
characterization of cubic and star-shaped dendritic pbs structures synthesized by a solvothermal method |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-84862158360&partnerID=40&md5=d727f2516407a6edc52bb0a46df11109 http://cmuir.cmu.ac.th/handle/6653943832/6733 |
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1681420669009526784 |