Synthesis of CuS with different morphologies by refluxing method: Nanopaticles in clusters and nanoflakes in spongelike clusters
Clusters of CuS nanoparticles and sponge-like structures of CuS nanoflakes were synthesized by refluxing method at a temperature of 130 °C for 1.5-6 h using copper chloride (CuCl 2·4H 2O) and thioacetamide (CH 3CSNH 2) as starting materials in deionized water to form [Cu(CH 3CSNH 2) 2]Cl 2 complexes...
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| Main Authors: | , , , |
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| Format: | Letter |
| Language: | English |
| Published: |
2014
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| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-84868324001&partnerID=40&md5=c0cac404f8cca808c3f3b4337d1792b9 http://cmuir.cmu.ac.th/handle/6653943832/6952 |
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| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | Clusters of CuS nanoparticles and sponge-like structures of CuS nanoflakes were synthesized by refluxing method at a temperature of 130 °C for 1.5-6 h using copper chloride (CuCl 2·4H 2O) and thioacetamide (CH 3CSNH 2) as starting materials in deionized water to form [Cu(CH 3CSNH 2) 2]Cl 2 complexes, specified by thermogravimetric, CHNS/O and Fourier transform inferred analyses. Phase and morphology were investigated by powder X-ray diffraction and scanning electron microscopy. |
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