One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites
Zn4Sb3 nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-...
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th-cmuir.6653943832-72412014-08-30T03:51:44Z One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites Sitthichai S. Thongtem T. Thongtem S. Suriwong T. Zn4Sb3 nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-ray (EDX) spectroscopy, transmission electron microscopy (TEM), Raman spectroscopy and UV-visible spectroscopy. In this research, Zn 4Sb3 nanocrystals with a prominent vibration mode at 144 cm-1 and 1.22 eV optical band gap were detected, including Zn 4Sb3-ZnSb composites were also synthesized using microwave plasma for 10 min. © 2013 Elsevier Ltd. All rights reserved. 2014-08-30T03:51:44Z 2014-08-30T03:51:44Z 2013 Article 07496036 10.1016/j.spmi.2013.10.004 SUMIE http://www.scopus.com/inward/record.url?eid=2-s2.0-84887095364&partnerID=40&md5=ee6854cc15fd4eb8c8c84d0f0c88018e http://cmuir.cmu.ac.th/handle/6653943832/7241 English |
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Zn4Sb3 nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-ray (EDX) spectroscopy, transmission electron microscopy (TEM), Raman spectroscopy and UV-visible spectroscopy. In this research, Zn 4Sb3 nanocrystals with a prominent vibration mode at 144 cm-1 and 1.22 eV optical band gap were detected, including Zn 4Sb3-ZnSb composites were also synthesized using microwave plasma for 10 min. © 2013 Elsevier Ltd. All rights reserved. |
| format |
Article |
| author |
Sitthichai S. Thongtem T. Thongtem S. Suriwong T. |
| spellingShingle |
Sitthichai S. Thongtem T. Thongtem S. Suriwong T. One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites |
| author_facet |
Sitthichai S. Thongtem T. Thongtem S. Suriwong T. |
| author_sort |
Sitthichai S. |
| title |
One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites |
| title_short |
One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites |
| title_full |
One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites |
| title_fullStr |
One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites |
| title_full_unstemmed |
One-step synthesis of Zn4Sb3 nanocrystals and Zn 4Sb3-ZnSb composites |
| title_sort |
one-step synthesis of zn4sb3 nanocrystals and zn 4sb3-znsb composites |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-84887095364&partnerID=40&md5=ee6854cc15fd4eb8c8c84d0f0c88018e http://cmuir.cmu.ac.th/handle/6653943832/7241 |
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1681420763581644800 |