Mechanical alloying of Sm and Fe mixtures having the molar ratio of 1/2 and 1/3
The mechanical alloying of Sm-Fe mixtures of molar ratios 1/2 and 1/3 were carried out. The milled mixtures were subjected to a two-step annealing process; first annealing for 1 h at 900 °C in argon gas, followed by a second annealing for 4 h at temperatures between 300 and 450 °C (Ta2) in nitrogen...
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| Main Authors: | , , |
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| Format: | Article |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://repository.li.mahidol.ac.th/handle/123456789/25940 |
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| Institution: | Mahidol University |
| Summary: | The mechanical alloying of Sm-Fe mixtures of molar ratios 1/2 and 1/3 were carried out. The milled mixtures were subjected to a two-step annealing process; first annealing for 1 h at 900 °C in argon gas, followed by a second annealing for 4 h at temperatures between 300 and 450 °C (Ta2) in nitrogen gas. Both the X-ray diffraction (XRD) and Moessbauer studies indicate that heat treatment of both mixtures results in the growth of the 2-17 (Sm2Fe17Nx) intermetallic. The coercivity of both milled mixtures increases as Ta2is raised, while the specific magnetization of both are seen to decrease initially and then increase as Ta2is raised further. |
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