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The basic principle of instrument for measuring concentrate of ammoniac within water is light absorption by ammoniac solution. Chemical cluster of ammoniac absorb advance light in range 990-1000 nm (infrared) length of waves theoretically. <br /> <br /> <br /> Indophenols...
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Format: | Final Project |
Language: | Indonesia |
Online Access: | https://digilib.itb.ac.id/gdl/view/16091 |
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Institution: | Institut Teknologi Bandung |
Language: | Indonesia |
Summary: | The basic principle of instrument for measuring concentrate of ammoniac within water is light absorption by ammoniac solution. Chemical cluster of ammoniac absorb advance light in range 990-1000 nm (infrared) length of waves theoretically. <br />
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Indophenols blue method used in this research so that length measurement of light waves can be done. Indophenols blue solution is alkali solution with pH 10, 4-11, 5 formed in existence of ammonium ion allied with hypochlorite, which is forming monochloramine. Monochloramine , hypochlorite and phenol will perform indophenols , the blue colored solution. Then nitroprusside will used as catalyst. <br />
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This procedure will result NH4 + + ClO- + H2O HC12H6Cl2O2N reaction chemically. <br />
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Experiment held with make various kind of concentrate. There are 6 kind of concentrate, and went on dilute solution. Laser beam fall into solution in a cuvet, because a beam spreading after through cuvet so used positif lens to accumulate ligaht into fotodioda sensor. A light source ia Laser He-Ne λ= 632,8 nm. During experiments demand change time of heat, measerument of temperature, also change physical on solution condition. <br />
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In a experiment of result, contiuned by make a regresi equation from experiment result. In y = mx+b equation form. The final regression equation is y =-6.905 x + 9.4655 Validation solution have various kind of concentrate. There are eight kinds of concentrate. Each of concentrate tested to make certain about concentration value measurable (x=y-b/m). Maximum error in validation solution is 79 % which is match at 6 ppm ammoniac concentration.And minimum error 5 % when concentrate ammoniac reached 0.32 ppm. |
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