#TITLE_ALTERNATIVE#
Reaction of toluene with iodine in the presence of concentrated nitric acid followed by oxidation <br /> <br /> with potassium permanganate had been carried out. The aim of this research was to study the <br /> <br /> possibility of electrophylic aromatic substitution by iodi...
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| Format: | Final Project |
| Language: | Indonesia |
| Online Access: | https://digilib.itb.ac.id/gdl/view/29393 |
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| Institution: | Institut Teknologi Bandung |
| Language: | Indonesia |
| Summary: | Reaction of toluene with iodine in the presence of concentrated nitric acid followed by oxidation <br />
<br />
with potassium permanganate had been carried out. The aim of this research was to study the <br />
<br />
possibility of electrophylic aromatic substitution by iodine in the presence of nitric acid <br />
<br />
as reagent. In the first step, toluene, iodine and concentrated nitric acid were refluxed at 85 °C for <br />
<br />
15 hours resulted in orange liquid and yellowish solid products. After separation by filtration, <br />
<br />
the two products were subsequenly oxidized by potassium permanganate under basic condition <br />
<br />
which resulted in two while solid products with the yield of 13.4% and 2.3%, respectively. <br />
<br />
The two products were characterized by chromatographic, spectroscopic and color reaction <br />
<br />
methods as well as melting point determination. However the identity of the two products still <br />
<br />
cannot be determined. <br />
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