VALIDASI METODE ANALISIS RESIDU SPIRAMISIN DALAM UDANG SECARA HPLC DENGAN PREPARASI SAMPMEL SPE DAN KLT - PREPARATIF
The high performance liquid chromatographic determination of spiramycin used in shrimp has been develop. Separation was performed by using either tlc-preparative with acetonitrile:0,2% perchloric acid (2;3) AS mobile phase or SPE with asetone as mobile phase. The ec=xtract containing sprimaycin exam...
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Main Author: | |
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Format: | Theses and Dissertations NonPeerReviewed |
Language: | English |
Published: |
2004
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Subjects: | |
Online Access: | http://repository.unair.ac.id/57632/1/KK%20FF%2089%2004%20Rac%20v.pdf http://repository.unair.ac.id/57632/ http://lib.unair.ac.id |
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Institution: | Universitas Airlangga |
Language: | English |
Summary: | The high performance liquid chromatographic determination of spiramycin used in shrimp has been develop. Separation was performed by using either tlc-preparative with acetonitrile:0,2% perchloric acid (2;3) AS mobile phase or SPE with asetone as mobile phase. The ec=xtract containing sprimaycin examined by HPLC using a Hypersil BDS and a mobile phase of CH3OH. The limit of detection was 0,05 mg.ml and the limit of quantitation was 0,16mg/ml |
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