1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in bo...
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2008
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id-ugm-repo.279362016-04-23T13:01:10Z https://repository.ugm.ac.id/27936/ 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN AI-DOUH, Mohammed Hadi Chemical Science Organic Chemistry Organic Chemical Synthesis ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in both COCI3and acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz). Keywords: 1HNMR [Yogyakarta] : Universitas Gadjah Mada 2008 Article PeerReviewed AI-DOUH, Mohammed Hadi (2008) 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN. Jurnal i-lib UGM, VIII (3). (Unpublished) http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10999 |
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Chemical Science Organic Chemistry Organic Chemical Synthesis |
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Chemical Science Organic Chemistry Organic Chemical Synthesis AI-DOUH, Mohammed Hadi 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
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ABSTRACT
The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the
presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete
assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in both COCI3and
acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz).
Keywords: 1HNMR |
format |
Article PeerReviewed |
author |
AI-DOUH, Mohammed Hadi |
author_facet |
AI-DOUH, Mohammed Hadi |
author_sort |
AI-DOUH, Mohammed Hadi |
title |
1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
title_short |
1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
title_full |
1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
title_fullStr |
1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
title_full_unstemmed |
1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN |
title_sort |
1d and 2d nmr studies of benzyl o-v anillin |
publisher |
[Yogyakarta] : Universitas Gadjah Mada |
publishDate |
2008 |
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https://repository.ugm.ac.id/27936/ http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10999 |
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