1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN

ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in bo...

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Main Author: AI-DOUH, Mohammed Hadi
Format: Article PeerReviewed
Published: [Yogyakarta] : Universitas Gadjah Mada 2008
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Online Access:https://repository.ugm.ac.id/27936/
http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10999
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spelling id-ugm-repo.279362016-04-23T13:01:10Z https://repository.ugm.ac.id/27936/ 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN AI-DOUH, Mohammed Hadi Chemical Science Organic Chemistry Organic Chemical Synthesis ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in both COCI3and acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz). Keywords: 1HNMR [Yogyakarta] : Universitas Gadjah Mada 2008 Article PeerReviewed AI-DOUH, Mohammed Hadi (2008) 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN. Jurnal i-lib UGM, VIII (3). (Unpublished) http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10999
institution Universitas Gadjah Mada
building UGM Library
country Indonesia
collection Repository Civitas UGM
topic Chemical Science
Organic Chemistry
Organic Chemical Synthesis
spellingShingle Chemical Science
Organic Chemistry
Organic Chemical Synthesis
AI-DOUH, Mohammed Hadi
1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
description ABSTRACT The reaction of o-vanillin A with benzyl bromide B2 in acetone as the solvent and K2C03 as a base in the presence of tetra-~butYlammonium iodide (TBAI) as catalyst formed benzyl o-vanillin, C. The complete assignments of C using PROTON, APT, OEPT-135, COSY, NOESY, HMQC and HMBC NMR in both COCI3and acetone-d6 are discussed, and the coupling constants J are reported in Hertz (Hz). Keywords: 1HNMR
format Article
PeerReviewed
author AI-DOUH, Mohammed Hadi
author_facet AI-DOUH, Mohammed Hadi
author_sort AI-DOUH, Mohammed Hadi
title 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
title_short 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
title_full 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
title_fullStr 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
title_full_unstemmed 1D AND 2D NMR STUDIES OF BENZYL O-V ANILLIN
title_sort 1d and 2d nmr studies of benzyl o-v anillin
publisher [Yogyakarta] : Universitas Gadjah Mada
publishDate 2008
url https://repository.ugm.ac.id/27936/
http://i-lib.ugm.ac.id/jurnal/download.php?dataId=10999
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