SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR
Synthesisofcement-zeolitecompositegranulesandtheadsorption-desorptiontestofethanol/watermixturehavebeensuccessfullyconducted.Cement-zeolitecompositegranulesweremadebymanuallystirringthemixtureof5gramsofnaturalzeolite,2gramsofportlandcement,and4mLofdistilledwaterinaporcelaindisk.Thesuspensionwasforme...
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[Yogyakarta] : Universitas Gadjah Mada
2011
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id-ugm-repo.883072014-08-20T02:52:16Z https://repository.ugm.ac.id/88307/ SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR , KOMEYNI RUSBA, S.Si , Dr. Yateman Aryanto ETD Synthesisofcement-zeolitecompositegranulesandtheadsorption-desorptiontestofethanol/watermixturehavebeensuccessfullyconducted.Cement-zeolitecompositegranulesweremadebymanuallystirringthemixtureof5gramsofnaturalzeolite,2gramsofportlandcement,and4mLofdistilledwaterinaporcelaindisk.Thesuspensionwasformedasgranulesandwasallowedtobedryatroomtemperaturein5days.Cement-zeolitegranuleswerecharacterizedusinginfraredspectroscopy(FTIR)andX-raydiffraction(XRD)methods.Thecompressivestrengthofcement-zeolitecompositegranuleswasdeterminedusingmaterialtestingmachine.Adsorptioncapacitytestwascarriedoutbysoakingcompositegranulesinwaterfor24hoursandthencalculatingtheweightdifferenceofcompositeganulesbeforeandaftersoaking.Adsorptionanddesorptiontestwereconductedbydropping1mLethanol-watermixturewithvariousconcentrations(99.9%,90%,80%and75%(v/v))ofethanoloncompositegranulesanditsadsorption-desorptiontimewasthennoted. C haracterizationusingFTIRshowedthefunctionalgroupsofcement-zeolitecompositegranulefillersandthefunctionalgroupsindicatingtheformationofcalciumsilicatehydrate(CSH)fromthecementhydrationreaction.ResultsofanalysisusingX-raydiffractionconfirmedtheFTIRdatawhichwasmarkedbythepresenceofdiffractionpeaksofthecompositecement-zeolitegranulefillersandcementhydrationproducts(ettringite,jennite,andtobermorite).Thestudyofthezeoliteparticlesizeeffectonthequalityofthecompositegranulesshowedthatthecompositegranuleswithparticlesizeof400meshasthehighestwateradsorptioncapacity(31.39%)andforparticlesizeof80meshhasthehighestcompressivestrength(140.4863N).Thestudyontheinfluenceoftheamountofcementshowedthatthecompositegranulespreparedbymixing1gramofcementwith5gramsofzeolitehasthehihestwateradsorptioncapacity(35.5%).Thehighestcompressivestrength(119.5302N)wasachievedbythecompositegranulesmadewith5gramsofcement.Theresultofdesorptiontimetestshowedthattheethanoldesorptiontimewasmuchfasterthanthatthewater,andthistimedifferencewasthenusedasthebasisforseparationofethanol-watermixturewithoutheating. [Yogyakarta] : Universitas Gadjah Mada 2011 Thesis NonPeerReviewed , KOMEYNI RUSBA, S.Si and , Dr. Yateman Aryanto (2011) SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR. UNSPECIFIED thesis, UNSPECIFIED. http://etd.ugm.ac.id/index.php?mod=penelitian_detail&sub=PenelitianDetail&act=view&typ=html&buku_id=50294 |
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ETD , KOMEYNI RUSBA, S.Si , Dr. Yateman Aryanto SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR |
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Synthesisofcement-zeolitecompositegranulesandtheadsorption-desorptiontestofethanol/watermixturehavebeensuccessfullyconducted.Cement-zeolitecompositegranulesweremadebymanuallystirringthemixtureof5gramsofnaturalzeolite,2gramsofportlandcement,and4mLofdistilledwaterinaporcelaindisk.Thesuspensionwasformedasgranulesandwasallowedtobedryatroomtemperaturein5days.Cement-zeolitegranuleswerecharacterizedusinginfraredspectroscopy(FTIR)andX-raydiffraction(XRD)methods.Thecompressivestrengthofcement-zeolitecompositegranuleswasdeterminedusingmaterialtestingmachine.Adsorptioncapacitytestwascarriedoutbysoakingcompositegranulesinwaterfor24hoursandthencalculatingtheweightdifferenceofcompositeganulesbeforeandaftersoaking.Adsorptionanddesorptiontestwereconductedbydropping1mLethanol-watermixturewithvariousconcentrations(99.9%,90%,80%and75%(v/v))ofethanoloncompositegranulesanditsadsorption-desorptiontimewasthennoted.
C
haracterizationusingFTIRshowedthefunctionalgroupsofcement-zeolitecompositegranulefillersandthefunctionalgroupsindicatingtheformationofcalciumsilicatehydrate(CSH)fromthecementhydrationreaction.ResultsofanalysisusingX-raydiffractionconfirmedtheFTIRdatawhichwasmarkedbythepresenceofdiffractionpeaksofthecompositecement-zeolitegranulefillersandcementhydrationproducts(ettringite,jennite,andtobermorite).Thestudyofthezeoliteparticlesizeeffectonthequalityofthecompositegranulesshowedthatthecompositegranuleswithparticlesizeof400meshasthehighestwateradsorptioncapacity(31.39%)andforparticlesizeof80meshhasthehighestcompressivestrength(140.4863N).Thestudyontheinfluenceoftheamountofcementshowedthatthecompositegranulespreparedbymixing1gramofcementwith5gramsofzeolitehasthehihestwateradsorptioncapacity(35.5%).Thehighestcompressivestrength(119.5302N)wasachievedbythecompositegranulesmadewith5gramsofcement.Theresultofdesorptiontimetestshowedthattheethanoldesorptiontimewasmuchfasterthanthatthewater,andthistimedifferencewasthenusedasthebasisforseparationofethanol-watermixturewithoutheating. |
format |
Theses and Dissertations NonPeerReviewed |
author |
, KOMEYNI RUSBA, S.Si , Dr. Yateman Aryanto |
author_facet |
, KOMEYNI RUSBA, S.Si , Dr. Yateman Aryanto |
author_sort |
, KOMEYNI RUSBA, S.Si |
title |
SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR |
title_short |
SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR |
title_full |
SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR |
title_fullStr |
SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR |
title_full_unstemmed |
SINTESIS GRANULA KOMPOSIT SEMEN-ZEOLITDAN UJI ADSORPSI-DESORPSI CAMPURAN ETANOL-AIR |
title_sort |
sintesis granula komposit semen-zeolitdan uji adsorpsi-desorpsi campuran etanol-air |
publisher |
[Yogyakarta] : Universitas Gadjah Mada |
publishDate |
2011 |
url |
https://repository.ugm.ac.id/88307/ http://etd.ugm.ac.id/index.php?mod=penelitian_detail&sub=PenelitianDetail&act=view&typ=html&buku_id=50294 |
_version_ |
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