Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis
Pineapple crown leaf fiber (PCLF) is one of the major biomass wastes from pineapple processing plants. It consists mostly of carbohydrate polymers, such as cellulose, hemicellulose, and lignin. It can be further processed to form a more valuable and widely used nanocrystalline cellulose (NCC). This...
Saved in:
Main Authors: | , , , , , , , |
---|---|
Format: | Article |
Language: | English English |
Published: |
Multidisciplinary Digital Publishing Institute (MDPI)
2021
|
Subjects: | |
Online Access: | https://eprints.ums.edu.my/id/eprint/31851/1/Isolation%20and%20characterization%20of%20nanocrystalline%20cellulose%20isolated%20from%20pineapple%20crown%20.ABSTRACT.pdf https://eprints.ums.edu.my/id/eprint/31851/2/Isolation%20and%20Characterization%20of%20Nanocrystalline%20Cellulose.pdf https://eprints.ums.edu.my/id/eprint/31851/ https://www.mdpi.com/2073-4360/13/23/4188 https://doi.org/10.3390/polym13234188 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
Institution: | Universiti Malaysia Sabah |
Language: | English English |
id |
my.ums.eprints.31851 |
---|---|
record_format |
eprints |
spelling |
my.ums.eprints.318512022-03-15T03:42:57Z https://eprints.ums.edu.my/id/eprint/31851/ Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis Fitriani Fitriani Sri Aprilia Nasrul Arahman Muhammad Roil Bilad Amri Amin amriamin@abulyatama.ac.id Nurul Huda Jumardi Roslan TD920-934 Rural and farm sanitary engineering TS1-2301 Manufactures Pineapple crown leaf fiber (PCLF) is one of the major biomass wastes from pineapple processing plants. It consists mostly of carbohydrate polymers, such as cellulose, hemicellulose, and lignin. It can be further processed to form a more valuable and widely used nanocrystalline cellulose (NCC). This study investigates the effect of hydrolysis time on the properties of the produced NCC. The acid hydrolysis was conducted using 1 M of sulfuric acid at hydrolysis times of 1–3 h. The resulting NCCs were then characterized by their morphology, functional groups, crystallinity, thermal stability, elemental composition, and production yield. The results show that the NCC products had a rod-like particle structure and possessed a strong cellulose crystalline structure typically found in agricultural fiber-based cellulose. The highest NCC yield was obtained at 79.37% for one hour of hydrolysis. This NCC also displayed a higher decomposition temperature of 176.9 C. The overall findings suggest that PCLF-derived NCC has attractive properties for a variety of applications. Multidisciplinary Digital Publishing Institute (MDPI) 2021-11-30 Article PeerReviewed text en https://eprints.ums.edu.my/id/eprint/31851/1/Isolation%20and%20characterization%20of%20nanocrystalline%20cellulose%20isolated%20from%20pineapple%20crown%20.ABSTRACT.pdf text en https://eprints.ums.edu.my/id/eprint/31851/2/Isolation%20and%20Characterization%20of%20Nanocrystalline%20Cellulose.pdf Fitriani Fitriani and Sri Aprilia and Nasrul Arahman and Muhammad Roil Bilad and Amri Amin and amriamin@abulyatama.ac.id and Nurul Huda and Jumardi Roslan (2021) Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis. Polymers, 13. pp. 1-12. ISSN 2073-4360 https://www.mdpi.com/2073-4360/13/23/4188 https://doi.org/10.3390/polym13234188 |
institution |
Universiti Malaysia Sabah |
building |
UMS Library |
collection |
Institutional Repository |
continent |
Asia |
country |
Malaysia |
content_provider |
Universiti Malaysia Sabah |
content_source |
UMS Institutional Repository |
url_provider |
http://eprints.ums.edu.my/ |
language |
English English |
topic |
TD920-934 Rural and farm sanitary engineering TS1-2301 Manufactures |
spellingShingle |
TD920-934 Rural and farm sanitary engineering TS1-2301 Manufactures Fitriani Fitriani Sri Aprilia Nasrul Arahman Muhammad Roil Bilad Amri Amin amriamin@abulyatama.ac.id Nurul Huda Jumardi Roslan Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
description |
Pineapple crown leaf fiber (PCLF) is one of the major biomass wastes from pineapple processing plants. It consists mostly of carbohydrate polymers, such as cellulose, hemicellulose, and lignin. It can be further processed to form a more valuable and widely used nanocrystalline cellulose (NCC). This study investigates the effect of hydrolysis time on the properties of the produced NCC. The acid hydrolysis was conducted using 1 M of sulfuric acid at hydrolysis times of 1–3 h. The resulting NCCs were then characterized by their morphology, functional groups, crystallinity, thermal stability, elemental composition, and production yield. The results show that the NCC products had a rod-like particle structure and possessed a strong cellulose crystalline structure typically found in agricultural fiber-based cellulose. The highest NCC yield was obtained at 79.37% for one hour of hydrolysis. This NCC also displayed a higher decomposition temperature of 176.9 C. The overall findings suggest that PCLF-derived NCC has attractive properties for a variety of applications. |
format |
Article |
author |
Fitriani Fitriani Sri Aprilia Nasrul Arahman Muhammad Roil Bilad Amri Amin amriamin@abulyatama.ac.id Nurul Huda Jumardi Roslan |
author_facet |
Fitriani Fitriani Sri Aprilia Nasrul Arahman Muhammad Roil Bilad Amri Amin amriamin@abulyatama.ac.id Nurul Huda Jumardi Roslan |
author_sort |
Fitriani Fitriani |
title |
Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
title_short |
Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
title_full |
Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
title_fullStr |
Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
title_full_unstemmed |
Isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
title_sort |
isolation and characterization of nanocrystalline cellulose isolated from pineapple crown leaf fiber agricultural wastes using acid hydrolysis |
publisher |
Multidisciplinary Digital Publishing Institute (MDPI) |
publishDate |
2021 |
url |
https://eprints.ums.edu.my/id/eprint/31851/1/Isolation%20and%20characterization%20of%20nanocrystalline%20cellulose%20isolated%20from%20pineapple%20crown%20.ABSTRACT.pdf https://eprints.ums.edu.my/id/eprint/31851/2/Isolation%20and%20Characterization%20of%20Nanocrystalline%20Cellulose.pdf https://eprints.ums.edu.my/id/eprint/31851/ https://www.mdpi.com/2073-4360/13/23/4188 https://doi.org/10.3390/polym13234188 |
_version_ |
1760230947186278400 |