Confirmation of the structure of (±)-preisomide by total synthesis

The structure of preisomide has been confirmed by total synthesis involving chemoselective oxazine formation and vinyl iodide carbonylation in six steps (longest linear sequence) and 23% overall yield.

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Main Authors:	Teo, Hong Kang, Sae-Lao, Patcharaporn, Bates, Roderick Wayland
Other Authors:	School of Chemistry, Chemical Engineering and Biotechnology
Format:	Article
Language:	English
Published:	2024
Subjects:	Chemistry Chemoselective Linear sequence
Online Access:	https://hdl.handle.net/10356/173471
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Institution:	Nanyang Technological University
Language:	English

id	sg-ntu-dr.10356-173471
record_format	dspace
spelling	sg-ntu-dr.10356-1734712024-12-06T15:32:32Z Confirmation of the structure of (±)-preisomide by total synthesis Teo, Hong Kang Sae-Lao, Patcharaporn Bates, Roderick Wayland School of Chemistry, Chemical Engineering and Biotechnology Chemistry Chemoselective Linear sequence The structure of preisomide has been confirmed by total synthesis involving chemoselective oxazine formation and vinyl iodide carbonylation in six steps (longest linear sequence) and 23% overall yield. Ministry of Education (MOE) Nanyang Technological University Submitted/Accepted version We thank NTU and the Singapore Ministry of Education (grant MOE-T2EP10221-0003) for support of this work. 2024-02-06T06:03:46Z 2024-02-06T06:03:46Z 2023 Journal Article Teo, H. K., Sae-Lao, P. & Bates, R. W. (2023). Confirmation of the structure of (±)-preisomide by total synthesis. Organic and Biomolecular Chemistry, 21(39), 7954-7959. https://dx.doi.org/10.1039/d3ob01250f 1477-0520 https://hdl.handle.net/10356/173471 10.1039/d3ob01250f 37750032 2-s2.0-85173916056 39 21 7954 7959 en MOE-T2EP10221-0003 Organic and Biomolecular Chemistry © 2023 The Authors. Published by The Royal Society of Chemistry. All rights reserved. This article may be downloaded for personal use only. Any other use requires prior permission of the copyright holder. The Version of Record is available online at http://doi.org/10.1039/d3ob01250f. application/pdf
institution	Nanyang Technological University
building	NTU Library
continent	Asia
country	Singapore Singapore
content_provider	NTU Library
collection	DR-NTU
language	English
topic	Chemistry Chemoselective Linear sequence
spellingShingle	Chemistry Chemoselective Linear sequence Teo, Hong Kang Sae-Lao, Patcharaporn Bates, Roderick Wayland Confirmation of the structure of (±)-preisomide by total synthesis
description	The structure of preisomide has been confirmed by total synthesis involving chemoselective oxazine formation and vinyl iodide carbonylation in six steps (longest linear sequence) and 23% overall yield.
author2	School of Chemistry, Chemical Engineering and Biotechnology
author_facet	School of Chemistry, Chemical Engineering and Biotechnology Teo, Hong Kang Sae-Lao, Patcharaporn Bates, Roderick Wayland
format	Article
author	Teo, Hong Kang Sae-Lao, Patcharaporn Bates, Roderick Wayland
author_sort	Teo, Hong Kang
title	Confirmation of the structure of (±)-preisomide by total synthesis
title_short	Confirmation of the structure of (±)-preisomide by total synthesis
title_full	Confirmation of the structure of (±)-preisomide by total synthesis
title_fullStr	Confirmation of the structure of (±)-preisomide by total synthesis
title_full_unstemmed	Confirmation of the structure of (±)-preisomide by total synthesis
title_sort	confirmation of the structure of (±)-preisomide by total synthesis
publishDate	2024
url	https://hdl.handle.net/10356/173471
_version_	1819113053639147520

Confirmation of the structure of (±)-preisomide by total synthesis

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