Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate (Na 2 S 2 O 3 ) in ethylene glycol (...
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| Main Authors: | , , |
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| Format: | Journal |
| Published: |
2017
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| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/42785 |
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| Institution: | Chiang Mai University |
| Summary: | Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate (Na 2 S 2 O 3 ) in ethylene glycol (EG) containing different contents of cetyltrimethylammonium bromide (CTAB) as a template and splitting agent by the 600 W cyclic microwave radiation (CMR). X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy and photoluminescence (PL) spectroscopy revealed the presence of only orthorhombic Sb 2 S 3 phase in the shape of twin flowers of single crystalline square nanorod petals, growing along the [001] direction, including the vibration peaks that were in accordance with those of the stibnite with the 435 nm violet wavelength emission peaks. |
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