Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent

Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate (Na 2 S 2 O 3 ) in ethylene glycol (...

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Main Authors:	Kavinchan J., Thongtem T., Thongtem S.
Format:	Journal
Published:	2017
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/42785
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-42785
record_format	dspace
spelling	th-cmuir.6653943832-427852017-09-28T06:39:05Z Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent Kavinchan J. Thongtem T. Thongtem S. Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate (Na 2 S 2 O 3 ) in ethylene glycol (EG) containing different contents of cetyltrimethylammonium bromide (CTAB) as a template and splitting agent by the 600 W cyclic microwave radiation (CMR). X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy and photoluminescence (PL) spectroscopy revealed the presence of only orthorhombic Sb 2 S 3 phase in the shape of twin flowers of single crystalline square nanorod petals, growing along the [001] direction, including the vibration peaks that were in accordance with those of the stibnite with the 435 nm violet wavelength emission peaks. 2017-09-28T06:39:05Z 2017-09-28T06:39:05Z 2012-09-01 Journal 15848663 2-s2.0-84866393300 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/42785
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
description	Antimony sulfide (Sb 2 S 3 ) was successfully synthesized from antimony chloride (SbCl 3 ) and sodium thiosulfate (Na 2 S 2 O 3 ) in ethylene glycol (EG) containing different contents of cetyltrimethylammonium bromide (CTAB) as a template and splitting agent by the 600 W cyclic microwave radiation (CMR). X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy and photoluminescence (PL) spectroscopy revealed the presence of only orthorhombic Sb 2 S 3 phase in the shape of twin flowers of single crystalline square nanorod petals, growing along the [001] direction, including the vibration peaks that were in accordance with those of the stibnite with the 435 nm violet wavelength emission peaks.
format	Journal
author	Kavinchan J. Thongtem T. Thongtem S.
spellingShingle	Kavinchan J. Thongtem T. Thongtem S. Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
author_facet	Kavinchan J. Thongtem T. Thongtem S.
author_sort	Kavinchan J.
title	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_short	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_full	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_fullStr	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_full_unstemmed	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_sort	cyclic microwave assisted synthesis of sb 2s 3 twin flowers in solutions containing a template and splitting agent
publishDate	2017
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/42785
_version_	1681422255337242624

Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent

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