Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method
Different morphologies of Bi2S3 nanostructures were synthesized by a 180°C and 12 h solvothermal reaction of solutions containing Bi(NOmiddot;5H and thioacetamide (CHSNH in diethylene glycol (DEG) as a solvent. The as-synthesized Bi2S3 products characterized by XRD, Raman spectroscopy, SEM, and TEM...
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| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
2014
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| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-84893760306&partnerID=40&md5=c33749fccb94dba4f5d98a10956c4771 http://cmuir.cmu.ac.th/handle/6653943832/4762 |
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| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | Different morphologies of Bi2S3 nanostructures were synthesized by a 180°C and 12 h solvothermal reaction of solutions containing Bi(NOmiddot;5H and thioacetamide (CHSNH in diethylene glycol (DEG) as a solvent. The as-synthesized Bi2S3 products characterized by XRD, Raman spectroscopy, SEM, and TEM showed that they were well-crystallized orthorhombic Bi2S3 phase with morphologies of nanorod-like, sheaf-like, carnation-like, and microspherical, controlled by different contents of polyvinylpyrrolidone (PVP) in the solutions. Based on the experimental results, a growth mechanism was also proposed and discussed. © 2013 Anukorn Phuruangrat et al. |
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