Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method
Different morphologies of Bi2S3 nanostructures were synthesized by a 180°C and 12 h solvothermal reaction of solutions containing Bi(NOmiddot;5H and thioacetamide (CHSNH in diethylene glycol (DEG) as a solvent. The as-synthesized Bi2S3 products characterized by XRD, Raman spectroscopy, SEM, and TEM...
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th-cmuir.6653943832-47622014-08-30T02:55:44Z Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method Phuruangrat A. Thongtem T. Thongtem S. Different morphologies of Bi2S3 nanostructures were synthesized by a 180°C and 12 h solvothermal reaction of solutions containing Bi(NOmiddot;5H and thioacetamide (CHSNH in diethylene glycol (DEG) as a solvent. The as-synthesized Bi2S3 products characterized by XRD, Raman spectroscopy, SEM, and TEM showed that they were well-crystallized orthorhombic Bi2S3 phase with morphologies of nanorod-like, sheaf-like, carnation-like, and microspherical, controlled by different contents of polyvinylpyrrolidone (PVP) in the solutions. Based on the experimental results, a growth mechanism was also proposed and discussed. © 2013 Anukorn Phuruangrat et al. 2014-08-30T02:55:44Z 2014-08-30T02:55:44Z 2013 Article 16874110 10.1155/2013/314012 http://www.scopus.com/inward/record.url?eid=2-s2.0-84893760306&partnerID=40&md5=c33749fccb94dba4f5d98a10956c4771 http://cmuir.cmu.ac.th/handle/6653943832/4762 English |
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Different morphologies of Bi2S3 nanostructures were synthesized by a 180°C and 12 h solvothermal reaction of solutions containing Bi(NOmiddot;5H and thioacetamide (CHSNH in diethylene glycol (DEG) as a solvent. The as-synthesized Bi2S3 products characterized by XRD, Raman spectroscopy, SEM, and TEM showed that they were well-crystallized orthorhombic Bi2S3 phase with morphologies of nanorod-like, sheaf-like, carnation-like, and microspherical, controlled by different contents of polyvinylpyrrolidone (PVP) in the solutions. Based on the experimental results, a growth mechanism was also proposed and discussed. © 2013 Anukorn Phuruangrat et al. |
| format |
Article |
| author |
Phuruangrat A. Thongtem T. Thongtem S. |
| spellingShingle |
Phuruangrat A. Thongtem T. Thongtem S. Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method |
| author_facet |
Phuruangrat A. Thongtem T. Thongtem S. |
| author_sort |
Phuruangrat A. |
| title |
Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method |
| title_short |
Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method |
| title_full |
Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method |
| title_fullStr |
Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method |
| title_full_unstemmed |
Influence of PVP on the morphologies of Bi2S3 nanostructures synthesized by solvothermal method |
| title_sort |
influence of pvp on the morphologies of bi2s3 nanostructures synthesized by solvothermal method |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-84893760306&partnerID=40&md5=c33749fccb94dba4f5d98a10956c4771 http://cmuir.cmu.ac.th/handle/6653943832/4762 |
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