Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders

Nano- to micron-sized powders of PZT and PLZT were hydrothermally synthesized at temperatures of 125 and 140°C, pressures of 500 and 600 kPa, and holding times of 3 and 5 h. It was found that calcining the as-synthesized materials at 800°C for 2 h produced fine spherical powders (200...300 nm) of PZ...

Full description

Saved in:
Bibliographic Details
Main Authors: Nualpralaksana S., Phanichphant S., Hengst M., Heimann R.B.
Format: Article
Language:German; English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-0035338828&partnerID=40&md5=a12235e8f4d5666d2456a6c3d825db54
http://cmuir.cmu.ac.th/handle/6653943832/4980
Tags: Add Tag
No Tags, Be the first to tag this record!
Institution: Chiang Mai University
Language: German; English
id th-cmuir.6653943832-4980
record_format dspace
spelling th-cmuir.6653943832-49802014-08-30T02:56:01Z Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders Nualpralaksana S. Phanichphant S. Hengst M. Heimann R.B. Nano- to micron-sized powders of PZT and PLZT were hydrothermally synthesized at temperatures of 125 and 140°C, pressures of 500 and 600 kPa, and holding times of 3 and 5 h. It was found that calcining the as-synthesized materials at 800°C for 2 h produced fine spherical powders (200...300 nm) of PZT with a 1:1 mass ratio of a rhombohedral PbZr0,58Ti0,42O3 and a tetragonal PbZr0,52Ti0,48O3 phase as well as powders (100...1 000 nm) of PLZT with a 2:1 mass ratio of a tetragonal (Pb,La) (Zr0,52Ti0,48)O3 and a cubic (Pb0,9La0,1) (Zr0,65Ti0,35)O3 phase. 2014-08-30T02:56:01Z 2014-08-30T02:56:01Z 2001 Article 01739913 CCFDD http://www.scopus.com/inward/record.url?eid=2-s2.0-0035338828&partnerID=40&md5=a12235e8f4d5666d2456a6c3d825db54 http://cmuir.cmu.ac.th/handle/6653943832/4980 German; English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language German; English
description Nano- to micron-sized powders of PZT and PLZT were hydrothermally synthesized at temperatures of 125 and 140°C, pressures of 500 and 600 kPa, and holding times of 3 and 5 h. It was found that calcining the as-synthesized materials at 800°C for 2 h produced fine spherical powders (200...300 nm) of PZT with a 1:1 mass ratio of a rhombohedral PbZr0,58Ti0,42O3 and a tetragonal PbZr0,52Ti0,48O3 phase as well as powders (100...1 000 nm) of PLZT with a 2:1 mass ratio of a tetragonal (Pb,La) (Zr0,52Ti0,48)O3 and a cubic (Pb0,9La0,1) (Zr0,65Ti0,35)O3 phase.
format Article
author Nualpralaksana S.
Phanichphant S.
Hengst M.
Heimann R.B.
spellingShingle Nualpralaksana S.
Phanichphant S.
Hengst M.
Heimann R.B.
Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders
author_facet Nualpralaksana S.
Phanichphant S.
Hengst M.
Heimann R.B.
author_sort Nualpralaksana S.
title Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders
title_short Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders
title_full Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders
title_fullStr Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders
title_full_unstemmed Hydrothermal synthesis of lead zirconate titanate (PZT) and lead lanthanum zirconate titanate (PLZT) nanopowders
title_sort hydrothermal synthesis of lead zirconate titanate (pzt) and lead lanthanum zirconate titanate (plzt) nanopowders
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-0035338828&partnerID=40&md5=a12235e8f4d5666d2456a6c3d825db54
http://cmuir.cmu.ac.th/handle/6653943832/4980
_version_ 1681420338950307840