Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles
Bi2S3nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3has the orthorhombic...
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th-cmuir.6653943832-508092018-09-04T04:48:20Z Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles Titipun Thongtem Chalermchai Pilapong Jutarat Kavinchan Anukorn Phuruangrat Somchai Thongtem Engineering Materials Science Bi2S3nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3has the orthorhombic phase and appears as nanorods in flower-shaped bundles. A transmission electron microscopic (TEM) study reveals the independent single Bi2S3nanorods with their growth along the [0 0 1] direction. A possible formation mechanism of Bi2S3nanorods in flower-shaped bundles is also proposed and discussed. Their UVvis spectrum shows the absorbance at 596 nm, with its direct energy band gap of 1.82 eV. © 2009 Elsevier B.V. 2018-09-04T04:46:02Z 2018-09-04T04:46:02Z 2010-06-25 Journal 09258388 2-s2.0-77954217737 10.1016/j.jallcom.2010.03.240 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77954217737&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50809 |
| institution |
Chiang Mai University |
| building |
Chiang Mai University Library |
| country |
Thailand |
| collection |
CMU Intellectual Repository |
| topic |
Engineering Materials Science |
| spellingShingle |
Engineering Materials Science Titipun Thongtem Chalermchai Pilapong Jutarat Kavinchan Anukorn Phuruangrat Somchai Thongtem Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| description |
Bi2S3nanorods in flower-shaped bundles were successfully synthesized from the decomposition of Bithiourea complexes under the microwave-assisted hydrothermal process. X-ray powder diffraction (XRD) patterns and field emission scanning electron microscopy (FE-SEM) show that Bi2S3has the orthorhombic phase and appears as nanorods in flower-shaped bundles. A transmission electron microscopic (TEM) study reveals the independent single Bi2S3nanorods with their growth along the [0 0 1] direction. A possible formation mechanism of Bi2S3nanorods in flower-shaped bundles is also proposed and discussed. Their UVvis spectrum shows the absorbance at 596 nm, with its direct energy band gap of 1.82 eV. © 2009 Elsevier B.V. |
| format |
Journal |
| author |
Titipun Thongtem Chalermchai Pilapong Jutarat Kavinchan Anukorn Phuruangrat Somchai Thongtem |
| author_facet |
Titipun Thongtem Chalermchai Pilapong Jutarat Kavinchan Anukorn Phuruangrat Somchai Thongtem |
| author_sort |
Titipun Thongtem |
| title |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_short |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_full |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_fullStr |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_full_unstemmed |
Microwave-assisted hydrothermal synthesis of Bi2S3 nanorods in flower-shaped bundles |
| title_sort |
microwave-assisted hydrothermal synthesis of bi2s3 nanorods in flower-shaped bundles |
| publishDate |
2018 |
| url |
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=77954217737&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/50809 |
| _version_ |
1681423656664694784 |