Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electro...
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| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
2014
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| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-48349116217&partnerID=40&md5=9e35b12728633cc67cfd40c04c639dd1 http://cmuir.cmu.ac.th/handle/6653943832/5497 |
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| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electron microscope (SEM), a transmission electron microscope (TEM), a selected area electron diffraction (SAED) technique and an energy dispersive X-ray (EDX) analyzer. In addition, a Raman spectrometer revealed the presence of the first and second overtone modes at 436 and 602 cm-1, respectively. Emission spectra of the products were detected at 412 nm using a photoluminescence (PL) spectrometer. © 2007 Elsevier Ltd and Techna Group S.r.l. |
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