Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals

PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electro...

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Main Authors:	Thongtem T., Kaowphong S., Thongtem S.
Format:	Article
Language:	English
Published:	2014
Online Access:	http://www.scopus.com/inward/record.url?eid=2-s2.0-48349116217&partnerID=40&md5=9e35b12728633cc67cfd40c04c639dd1 http://cmuir.cmu.ac.th/handle/6653943832/5497
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Institution:	Chiang Mai University
Language:	English

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spelling	th-cmuir.6653943832-54972014-08-30T02:56:35Z Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals Thongtem T. Kaowphong S. Thongtem S. PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electron microscope (SEM), a transmission electron microscope (TEM), a selected area electron diffraction (SAED) technique and an energy dispersive X-ray (EDX) analyzer. In addition, a Raman spectrometer revealed the presence of the first and second overtone modes at 436 and 602 cm-1, respectively. Emission spectra of the products were detected at 412 nm using a photoluminescence (PL) spectrometer. © 2007 Elsevier Ltd and Techna Group S.r.l. 2014-08-30T02:56:35Z 2014-08-30T02:56:35Z 2008 Article 02728842 10.1016/j.ceramint.2007.05.007 CINND http://www.scopus.com/inward/record.url?eid=2-s2.0-48349116217&partnerID=40&md5=9e35b12728633cc67cfd40c04c639dd1 http://cmuir.cmu.ac.th/handle/6653943832/5497 English
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
language	English
description	PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electron microscope (SEM), a transmission electron microscope (TEM), a selected area electron diffraction (SAED) technique and an energy dispersive X-ray (EDX) analyzer. In addition, a Raman spectrometer revealed the presence of the first and second overtone modes at 436 and 602 cm-1, respectively. Emission spectra of the products were detected at 412 nm using a photoluminescence (PL) spectrometer. © 2007 Elsevier Ltd and Techna Group S.r.l.
format	Article
author	Thongtem T. Kaowphong S. Thongtem S.
spellingShingle	Thongtem T. Kaowphong S. Thongtem S. Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
author_facet	Thongtem T. Kaowphong S. Thongtem S.
author_sort	Thongtem T.
title	Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_short	Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_full	Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_fullStr	Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_full_unstemmed	Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_sort	biomolecule and surfactant-assisted hydrothermal synthesis of pbs crystals
publishDate	2014
url	http://www.scopus.com/inward/record.url?eid=2-s2.0-48349116217&partnerID=40&md5=9e35b12728633cc67cfd40c04c639dd1 http://cmuir.cmu.ac.th/handle/6653943832/5497
_version_	1681420436866334720

Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals

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