Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) wit...
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
2014
|
| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-51249089427&partnerID=40&md5=4b7d480f74cee4da97b9069afda5a206 http://cmuir.cmu.ac.th/handle/6653943832/5968 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) with flower-like, hollow spherical, and tubular structures were detected, and had the same vibration wavenumber at 474 cm-1. They displayed two emission peaks at 411, and 432 nm. The formation of CuS with different morphologies was proposed according to the analytical results. © 2008 Elsevier B.V. All rights reserved. |
|---|