Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) wit...
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th-cmuir.6653943832-59682014-08-30T03:23:41Z Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process Thongtem T. Phuruangrat A. Thongtem S. CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) with flower-like, hollow spherical, and tubular structures were detected, and had the same vibration wavenumber at 474 cm-1. They displayed two emission peaks at 411, and 432 nm. The formation of CuS with different morphologies was proposed according to the analytical results. © 2008 Elsevier B.V. All rights reserved. 2014-08-30T03:23:41Z 2014-08-30T03:23:41Z 2009 Article 15671739 10.1016/j.cap.2008.01.011 http://www.scopus.com/inward/record.url?eid=2-s2.0-51249089427&partnerID=40&md5=4b7d480f74cee4da97b9069afda5a206 http://cmuir.cmu.ac.th/handle/6653943832/5968 English |
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CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) with flower-like, hollow spherical, and tubular structures were detected, and had the same vibration wavenumber at 474 cm-1. They displayed two emission peaks at 411, and 432 nm. The formation of CuS with different morphologies was proposed according to the analytical results. © 2008 Elsevier B.V. All rights reserved. |
format |
Article |
author |
Thongtem T. Phuruangrat A. Thongtem S. |
spellingShingle |
Thongtem T. Phuruangrat A. Thongtem S. Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
author_facet |
Thongtem T. Phuruangrat A. Thongtem S. |
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Thongtem T. |
title |
Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
title_short |
Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
title_full |
Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
title_fullStr |
Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
title_full_unstemmed |
Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
title_sort |
formation of cus with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process |
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2014 |
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http://www.scopus.com/inward/record.url?eid=2-s2.0-51249089427&partnerID=40&md5=4b7d480f74cee4da97b9069afda5a206 http://cmuir.cmu.ac.th/handle/6653943832/5968 |
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