Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process

CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) wit...

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Main Authors: Thongtem T., Phuruangrat A., Thongtem S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-51249089427&partnerID=40&md5=4b7d480f74cee4da97b9069afda5a206
http://cmuir.cmu.ac.th/handle/6653943832/5968
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-59682014-08-30T03:23:41Z Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process Thongtem T. Phuruangrat A. Thongtem S. CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) with flower-like, hollow spherical, and tubular structures were detected, and had the same vibration wavenumber at 474 cm-1. They displayed two emission peaks at 411, and 432 nm. The formation of CuS with different morphologies was proposed according to the analytical results. © 2008 Elsevier B.V. All rights reserved. 2014-08-30T03:23:41Z 2014-08-30T03:23:41Z 2009 Article 15671739 10.1016/j.cap.2008.01.011 http://www.scopus.com/inward/record.url?eid=2-s2.0-51249089427&partnerID=40&md5=4b7d480f74cee4da97b9069afda5a206 http://cmuir.cmu.ac.th/handle/6653943832/5968 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description CuCl2 · 2H2O and CH3CSNH2 were dissolved in ethylene glycol, and followed by the addition of NaOH to form solutions with different pH values. Reactions proceeded in surfactant-free solutions contained in an acid digestion bomb using a microwave irradiation at different conditions. Pure CuS (hcp) with flower-like, hollow spherical, and tubular structures were detected, and had the same vibration wavenumber at 474 cm-1. They displayed two emission peaks at 411, and 432 nm. The formation of CuS with different morphologies was proposed according to the analytical results. © 2008 Elsevier B.V. All rights reserved.
format Article
author Thongtem T.
Phuruangrat A.
Thongtem S.
spellingShingle Thongtem T.
Phuruangrat A.
Thongtem S.
Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
author_facet Thongtem T.
Phuruangrat A.
Thongtem S.
author_sort Thongtem T.
title Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
title_short Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
title_full Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
title_fullStr Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
title_full_unstemmed Formation of CuS with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
title_sort formation of cus with flower-like, hollow spherical, and tubular structures using the solvothermal-microwave process
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-51249089427&partnerID=40&md5=4b7d480f74cee4da97b9069afda5a206
http://cmuir.cmu.ac.th/handle/6653943832/5968
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