Preparation of flower-like PbS nano-structures using cyclic microwave radiation
Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The...
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Journal |
| Published: |
2018
|
| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=53249107976&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60496 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Chiang Mai University |
| Summary: | Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The experimental and simulated patterns are in good accord. A Raman spectrometer revealed the presence of vibrations at 134, 275 and 431 cm-1. Flower-like PbS nano-structures were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM), although the products were prepared using different mole ratios of the starting agents. |
|---|