Preparation of flower-like PbS nano-structures using cyclic microwave radiation

Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The...

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Main Authors:	Titipun Thongtem, Anukorn Phuruangrat, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Materials Science
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=53249107976&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60496
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-60496
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spelling	th-cmuir.6653943832-604962018-09-10T03:43:51Z Preparation of flower-like PbS nano-structures using cyclic microwave radiation Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem Materials Science Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The experimental and simulated patterns are in good accord. A Raman spectrometer revealed the presence of vibrations at 134, 275 and 431 cm-1. Flower-like PbS nano-structures were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM), although the products were prepared using different mole ratios of the starting agents. 2018-09-10T03:43:51Z 2018-09-10T03:43:51Z 2008-10-10 Journal 12299162 2-s2.0-53249107976 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=53249107976&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60496
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Materials Science
spellingShingle	Materials Science Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem Preparation of flower-like PbS nano-structures using cyclic microwave radiation
description	Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The experimental and simulated patterns are in good accord. A Raman spectrometer revealed the presence of vibrations at 134, 275 and 431 cm-1. Flower-like PbS nano-structures were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM), although the products were prepared using different mole ratios of the starting agents.
format	Journal
author	Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem
author_facet	Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem
author_sort	Titipun Thongtem
title	Preparation of flower-like PbS nano-structures using cyclic microwave radiation
title_short	Preparation of flower-like PbS nano-structures using cyclic microwave radiation
title_full	Preparation of flower-like PbS nano-structures using cyclic microwave radiation
title_fullStr	Preparation of flower-like PbS nano-structures using cyclic microwave radiation
title_full_unstemmed	Preparation of flower-like PbS nano-structures using cyclic microwave radiation
title_sort	preparation of flower-like pbs nano-structures using cyclic microwave radiation
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=53249107976&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60496
_version_	1681425446467534848

Preparation of flower-like PbS nano-structures using cyclic microwave radiation

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