Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods

PZT ceramics were prepared from a mixture of a mixed-oxide powder with the particles as large as 1 m, and a sol from a triol sol-gel method. The latter provided small particles of ∼20-100 nm after being calcined at 600°C. This mixture thus so called 'sol-bonded PZT powder'. The powder was...

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Bibliographic Details
Main Authors: Chontira Sangsubun, Anucha Watcharapasorn, Manoch Naksata, Tawee Tunkasiri, Sukanda Jiansirisomboon
Format: Journal
Published: 2018
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Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449114441&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/61158
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Institution: Chiang Mai University
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Summary:PZT ceramics were prepared from a mixture of a mixed-oxide powder with the particles as large as 1 m, and a sol from a triol sol-gel method. The latter provided small particles of ∼20-100 nm after being calcined at 600°C. This mixture thus so called 'sol-bonded PZT powder'. The powder was sintered at the temperature between 950-1200°C. X-ray diffraction results suggested that phases were changed from predominant rhombohedral to tetragonal with increasing the sintering temperature. The maximum room temperature dielectric constant of 1471 at 1 kHz could be achieved in the ceramic sintered at 1100°C, where the densification was optimized.