Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods

PZT ceramics were prepared from a mixture of a mixed-oxide powder with the particles as large as 1 m, and a sol from a triol sol-gel method. The latter provided small particles of ∼20-100 nm after being calcined at 600°C. This mixture thus so called 'sol-bonded PZT powder'. The powder was...

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Main Authors: Chontira Sangsubun, Anucha Watcharapasorn, Manoch Naksata, Tawee Tunkasiri, Sukanda Jiansirisomboon
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/61158
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-611582018-09-10T04:09:54Z Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods Chontira Sangsubun Anucha Watcharapasorn Manoch Naksata Tawee Tunkasiri Sukanda Jiansirisomboon Materials Science Physics and Astronomy PZT ceramics were prepared from a mixture of a mixed-oxide powder with the particles as large as 1 m, and a sol from a triol sol-gel method. The latter provided small particles of ∼20-100 nm after being calcined at 600°C. This mixture thus so called 'sol-bonded PZT powder'. The powder was sintered at the temperature between 950-1200°C. X-ray diffraction results suggested that phases were changed from predominant rhombohedral to tetragonal with increasing the sintering temperature. The maximum room temperature dielectric constant of 1471 at 1 kHz could be achieved in the ceramic sintered at 1100°C, where the densification was optimized. 2018-09-10T04:05:43Z 2018-09-10T04:05:43Z 2007-12-01 Journal 15635112 00150193 2-s2.0-75449114441 10.1080/00150190701512318 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449114441&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61158
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Materials Science
Physics and Astronomy
spellingShingle Materials Science
Physics and Astronomy
Chontira Sangsubun
Anucha Watcharapasorn
Manoch Naksata
Tawee Tunkasiri
Sukanda Jiansirisomboon
Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
description PZT ceramics were prepared from a mixture of a mixed-oxide powder with the particles as large as 1 m, and a sol from a triol sol-gel method. The latter provided small particles of ∼20-100 nm after being calcined at 600°C. This mixture thus so called 'sol-bonded PZT powder'. The powder was sintered at the temperature between 950-1200°C. X-ray diffraction results suggested that phases were changed from predominant rhombohedral to tetragonal with increasing the sintering temperature. The maximum room temperature dielectric constant of 1471 at 1 kHz could be achieved in the ceramic sintered at 1100°C, where the densification was optimized.
format Journal
author Chontira Sangsubun
Anucha Watcharapasorn
Manoch Naksata
Tawee Tunkasiri
Sukanda Jiansirisomboon
author_facet Chontira Sangsubun
Anucha Watcharapasorn
Manoch Naksata
Tawee Tunkasiri
Sukanda Jiansirisomboon
author_sort Chontira Sangsubun
title Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
title_short Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
title_full Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
title_fullStr Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
title_full_unstemmed Preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
title_sort preparation of sol-bonded lead zirconate titanate ceramics via sol-gel and mixed-oxide methods
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449114441&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/61158
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