Cost-effective flow injection spectrophotometric assay of iron content in pharmaceutical preparations using salicylate reagent

A new flow injection procedure for an assay of Fe(III) by using salicylate obtained from antipyretic powder, which is a cheap and easily available reagent, is proposed. A red complex was continuously monitored by a laboratory-made green LED colorimeter. A linear calibration was obtained in the range...

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Bibliographic Details
Main Authors: Udnan Y., Jakmunee J., Jayasavati S., Christian G.D., Synovec R.E., Grudpan K.
Format: Conference or Workshop Item
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-7044225834&partnerID=40&md5=34c48f9227186a46f5c036de102ac237
http://www.ncbi.nlm.nih.gov/pubmed/18969735
http://cmuir.cmu.ac.th/handle/6653943832/6246
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Institution: Chiang Mai University
Language: English
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Summary:A new flow injection procedure for an assay of Fe(III) by using salicylate obtained from antipyretic powder, which is a cheap and easily available reagent, is proposed. A red complex was continuously monitored by a laboratory-made green LED colorimeter. A linear calibration was obtained in the range of 1-20 mg Fe l-1 with a detection limit of 0.5 mg Fe l-1 and R.S.D.s of 1.4-5.4% (n=3, for 1-20 mg Fe l-1). The new procedure was applied to assay iron contents in pharmaceutical preparations. The results were in good agreement with those of the USP standard method. © 2004 Published by Elsevier B.V.