Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100-200 °C for 6-48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM...
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| Main Authors: | , , |
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| Format: | Conference or Workshop Item |
| Language: | English |
| Published: |
2014
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| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-77951660316&partnerID=40&md5=3e35a6e28ff210f05cb1d7df06ed3c62 http://cmuir.cmu.ac.th/handle/6653943832/6272 |
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| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100-200 °C for 6-48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb2S3 in the shape of spikes, with their growths in the [001] direction and Eg of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment. ©2010 IEEE. |
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