Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction

Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100-200 °C for 6-48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM...

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Main Authors: Pilapong C., Thongtem T., Thongtem S.
Format: Conference or Workshop Item
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-77951660316&partnerID=40&md5=3e35a6e28ff210f05cb1d7df06ed3c62
http://cmuir.cmu.ac.th/handle/6653943832/6272
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Institution: Chiang Mai University
Language: English
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spelling th-cmuir.6653943832-62722014-08-30T03:24:02Z Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction Pilapong C. Thongtem T. Thongtem S. Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100-200 °C for 6-48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb2S3 in the shape of spikes, with their growths in the [001] direction and Eg of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment. ©2010 IEEE. 2014-08-30T03:24:02Z 2014-08-30T03:24:02Z 2010 Conference Paper 9.78142E+12 10.1109/INEC.2010.5425105 80006 http://www.scopus.com/inward/record.url?eid=2-s2.0-77951660316&partnerID=40&md5=3e35a6e28ff210f05cb1d7df06ed3c62 http://cmuir.cmu.ac.th/handle/6653943832/6272 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description Spikes of Sb2S3 (antimony sulfide) were synthesized by hydrothermal reaction at 100-200 °C for 6-48 h. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), high resolution TEM (HRTEM) and UV-vis absorption spectroscopy, the products were specified as orthorhombic Sb2S3 in the shape of spikes, with their growths in the [001] direction and Eg of 5.40 eV. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment. ©2010 IEEE.
format Conference or Workshop Item
author Pilapong C.
Thongtem T.
Thongtem S.
spellingShingle Pilapong C.
Thongtem T.
Thongtem S.
Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
author_facet Pilapong C.
Thongtem T.
Thongtem S.
author_sort Pilapong C.
title Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
title_short Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
title_full Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
title_fullStr Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
title_full_unstemmed Large-scale synthesis of Sb2S3 spikes by hydrothermal reaction
title_sort large-scale synthesis of sb2s3 spikes by hydrothermal reaction
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-77951660316&partnerID=40&md5=3e35a6e28ff210f05cb1d7df06ed3c62
http://cmuir.cmu.ac.th/handle/6653943832/6272
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