Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
The solid-state mixed oxide method via a rapid vibro-milling technique was explored for the preparation of single-phase Zn2Nb34O 87 nanopowders. Phase formation of zinc niobate was investigated as a function of calcination temperature by using a combination of thermogravimetric/differential thermal...
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
2014
|
| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-84875961945&partnerID=40&md5=c603b42a6d975917da4b868c256384e7 http://cmuir.cmu.ac.th/handle/6653943832/7155 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | The solid-state mixed oxide method via a rapid vibro-milling technique was explored for the preparation of single-phase Zn2Nb34O 87 nanopowders. Phase formation of zinc niobate was investigated as a function of calcination temperature by using a combination of thermogravimetric/differential thermal analyzer (TG/DTA) and X-ray diffraction (XRD) techniques. Morphology, particle size and chemical composition of the powders were determined by scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) technique. The obtained results clearly revealed the influences of calcination temperature on phase formation and particle size of Zn2Nb34O87 nanopowder. © 2013 Elsevier B.V. All rights reserved. |
|---|