Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction

Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction

The solid-state mixed oxide method via a rapid vibro-milling technique was explored for the preparation of single-phase Zn2Nb34O 87 nanopowders. Phase formation of zinc niobate was investigated as a function of calcination temperature by using a combination of thermogravimetric/differential thermal...

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Main Authors: Amonpattaratkit P., Ananta S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-84875961945&partnerID=40&md5=c603b42a6d975917da4b868c256384e7
http://cmuir.cmu.ac.th/handle/6653943832/7155
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Language: English
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spelling th-cmuir.6653943832-71552014-08-30T03:51:38Z Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction Amonpattaratkit P. Ananta S. The solid-state mixed oxide method via a rapid vibro-milling technique was explored for the preparation of single-phase Zn2Nb34O 87 nanopowders. Phase formation of zinc niobate was investigated as a function of calcination temperature by using a combination of thermogravimetric/differential thermal analyzer (TG/DTA) and X-ray diffraction (XRD) techniques. Morphology, particle size and chemical composition of the powders were determined by scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) technique. The obtained results clearly revealed the influences of calcination temperature on phase formation and particle size of Zn2Nb34O87 nanopowder. © 2013 Elsevier B.V. All rights reserved. 2014-08-30T03:51:38Z 2014-08-30T03:51:38Z 2013 Article 02540584 10.1016/j.matchemphys.2013.01.039 MCHPD http://www.scopus.com/inward/record.url?eid=2-s2.0-84875961945&partnerID=40&md5=c603b42a6d975917da4b868c256384e7 http://cmuir.cmu.ac.th/handle/6653943832/7155 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description The solid-state mixed oxide method via a rapid vibro-milling technique was explored for the preparation of single-phase Zn2Nb34O 87 nanopowders. Phase formation of zinc niobate was investigated as a function of calcination temperature by using a combination of thermogravimetric/differential thermal analyzer (TG/DTA) and X-ray diffraction (XRD) techniques. Morphology, particle size and chemical composition of the powders were determined by scanning electron microscopy (SEM) and energy-dispersive X-ray (EDX) technique. The obtained results clearly revealed the influences of calcination temperature on phase formation and particle size of Zn2Nb34O87 nanopowder. © 2013 Elsevier B.V. All rights reserved.
format Article
author Amonpattaratkit P.
Ananta S.
spellingShingle Amonpattaratkit P.
Ananta S.
Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
author_facet Amonpattaratkit P.
Ananta S.
author_sort Amonpattaratkit P.
title Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
title_short Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
title_full Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
title_fullStr Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
title_full_unstemmed Effects of calcination temperature on phase formation and particle size of Zn2Nb34O87 powder synthesized by solid-state reaction
title_sort effects of calcination temperature on phase formation and particle size of zn2nb34o87 powder synthesized by solid-state reaction
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-84875961945&partnerID=40&md5=c603b42a6d975917da4b868c256384e7
http://cmuir.cmu.ac.th/handle/6653943832/7155
_version_ 1681420747695718400

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