C2 amination of pyridine with primary amines mediated by sodium hydride in the presence of lithium iodide
N-Butylpyridin-2-amine (3). An oven-dried, 250 mL three-necked roundbottomed flask fitted with a 25 x 15 mm Teflon-coated oval magnetic stir bar, a thermometer, rubber septum and a Liebig reflux condenser, is connected to a Schlenk line (Note 2). Sodium hydride (NaH) (3.00 g, 75.0 mmol, 3.0 equiv)...
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| Main Authors: | , , |
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| 格式: | Article |
| 語言: | English |
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2022
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| 在線閱讀: | https://hdl.handle.net/10356/154826 |
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| 機構: | Nanyang Technological University |
| 語言: | English |